Determination of halogenated hydrocarbons in urine samples using a needle trap device packed with Ni/Zn–BTC bi-MMOF via the dynamic headspace method
نویسندگان
چکیده
منابع مشابه
Rapid determination of light halogenated hydrocarbons in urine.
We describe a rapid method for determining light halogenated hydrocarbons (LHH) in urine by electron capture gas-liquid chromatography. The hydrocarbons are extracted from urine into pentane. A 2-microliter injection of the pentane extract provides a detection limit of less than 1 microgram/liter.
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Needle trap devices (NTDs) are a relatively new and promising tool for headspace (HS) analysis. In this study, a dynamic HS sampling procedure is evaluated for the determination of volatile organic compounds (VOCs) in whole blood samples. A full factorial design was used to evaluate the influence of the number of cycles and incubation time and it is demonstrated that the controlling factor in t...
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Introduction: Due to the widespread use of toxic chemicals in most workplaces that can lead to toxic effects on human, various chemical extraction technique have been defined for analysis these toxic substances in air, water and biological samples. The purpose of this research is extraction of toluene and methyl ethyl ketone from aquatic samples with needle trap device and one co...
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در سال های اخیر، تقاضای استفاده از تئوری خطی ویسکوالاستیسیته بیشتر شده است. با افزایش استفاده از کامپوزیت های پیشرفته در صنایع هوایی و همچنین استفاده روزافزون از مواد پلیمری، اهمیت روش های دقیق طراحی و تحلیل چنین ساختارهایی بیشتر شده است. این مواد جدید از خودشان رفتارهای مکانیکی ارائه می دهند که با تئوری های الاستیسیته و ویسکوزیته، نمی توان آن ها را توصیف کرد. این مواد، خواص ویسکوالاستیک دارند....
Development of a Method Based on the Needle-trap Microextraction Filled with Hydroxyapatite and Polyaniline Nanocomposite for Determination of Volatile Organic Compounds in the Air
In this study, the efficiency of packed needle trap with hydroxyapatite/polyaniline (NTD-HAP/PA) nanocomposite was assessed in air sampling and analysis of a hazardous group of VOCs such as benzene, toluene, ethylbenzene and xylenes. The effects of main parameters, including desorption temperature and time, were evaluated on the performance and carryover of prepared NTDs. Moreover, the repeatab...
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ژورنال
عنوان ژورنال: RSC Advances
سال: 2021
ISSN: 2046-2069
DOI: 10.1039/d1ra03227e